X-ray diffraction methods for high-pressure solid-state synthesis
Public DepositedMLA citation style (9th ed.)
Elsevier. 2022. marian.hykucommons.org/concern/generic_works/bb366e45-b3ec-4a02-b68a-68e16dbd72fd?q=12%2F18%2F1959%200%3A00. X-ray Diffraction Methods for High-pressure Solid-state Synthesis.APA citation style (7th ed.)
(2022). X-ray diffraction methods for high-pressure solid-state synthesis. https://marian.hykucommons.org/concern/generic_works/bb366e45-b3ec-4a02-b68a-68e16dbd72fd?q=12%2F18%2F1959%200%3A00Chicago citation style (CMOS 17, author-date)
X-Ray Diffraction Methods for High-Pressure Solid-State Synthesis. Elsevier. 2022. https://marian.hykucommons.org/concern/generic_works/bb366e45-b3ec-4a02-b68a-68e16dbd72fd?q=12%2F18%2F1959%200%3A00.Note: These citations are programmatically generated and may be incomplete.
This chapter provides a comprehensive overview of modern high pressure solid-state synthesis methods, with a specific focus on their integration with in situ X-ray diffraction methods. Fundamental concepts in solid-state synthesis are re-examined within the context of synthesis at high pressures, and additional considerations specific to high pressure are introduced. We examine three common apparatuses for achieving high pressures: the Paris–Edinburgh press, the diamond anvil cell, and the multi-anvil press. We present the advantages and disadvantages of each method in the context of high-pressure synthesis, using illustrative examples from the literature. We hope that this chapter will provide the curious solid-state chemist with the foundational understanding required to begin their foray into world of high-pressure synthesis.
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Reference Module in Chemistry, Molecular Sciences and Chemical Engineering
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